NMR Spectroscopy Service

Services

The NMR facility in the School of Mathematical and Physical Sciences is equipped with five instruments at 400MHz (4) and 500MHz (1), capable of performing a range of measurements, including:

• standard ¹H and ¹³C measurements
• multinuclear NMR (e.g. ²H, ¹¹B, ¹⁹F, ²⁹Si, ³¹P etc.)
• variable temperature (above and below ambient)
• 2D NMR (e.g. HSQC, HMBC, DOSY, etc.)
• routine solid state NMR 

We provide expert NMR services to both internal (School of Mathematical and Physical Sciences and other Schools) users, as well as external clients (other Universities, commercial customers).

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Instruments 

Bruker AVIIIHD 500MHz - "Millicent"

• 5mm solution state BBFO SmartProbe - 1H / 19F-15N dual resonance, z-gradient
• 4mm solid state 1H(19F) / 31P-15N dual resonance
• Bookable instrument for trained users

Bruker AVIIIHD 400MHz - "Magnus"

• 5mm solution state BBFO SmartProbe - 1H / 19F-15N dual resonance, z-gradient
• Open-access instrument for trained users

Bruker AVIII 400MHz - "Marmaduke"

• 5mm solution state BBFO - 1H / 19F-15N dual resonance, z-gradient
• Bookable instrument for trained users

Bruker AV 400 MHz - "Monty"

• 5 mm solution state BBFO SmartProbe - 1H / 19F-15N dual resonance, z-gradient
• Open-access instrument for trained users

Spinsolve 60 Benchtop NMR spectrometer

• 5 mm solution state probe 1H, 19F, 31P
• Flow cell for continuous reaction monitoring
• 20 position sample changer
• Open access instrument for undergraduate use in teaching labs

All instruments are equipped with 60-position sample changer for solution state samples.

Contact

To discuss your requirements please get in touch with our NMR specialist Dr Khalid Doudin.

Email: k.doudin@sheffield.ac.uk 
Phone: +44 (0)114 222 9312